History of Spectroscopy


L. spectrum - an appearance, an apparition, from spectare, to behold

G. skopein - to view

Spectroscopy is used to determine identity, quantity, structure, and the environment of atoms, molecules, and ions by analyzing the radiation emitted or absorbed by atoms, molecules, or ions.

Optical spectroscopy is concerned with transitions of valence electrons.

X-ray spectroscopy is concerned with the transition of inner-core electrons.

Nuclear magnetic spectroscopy is concerned with transitions involving the nucleus.

Mass spectrometry involves the separations of ions based on their mass.

SPECTROSCOPIC TIMELINE

Gen 1:3 "And God said 'Let there be light' "

Gen 9:13 "I set my bow in the clouds, and it shall be a sign ..."

423 B.C. use of the lens by Aristophanes

400 BC Aristotle recognizes that light was necessary for color to exist

300 BC Euclid discussed the focus of a spherical mirror

40 A.D. Seneca observed the light scattering properties of prisms

50 AD Cleomedes discussed the refraction of light

100 Ptolemy studied incidence and refraction.

139 Claudius Ptolemy made detailed tables on the reflection and refraction of light

~1010 Althazen described the planar nature of reflection

1038 Alhazen studied reflection and refraction of light

1250 Roger Bacon determined the focal points of concave mirror

~1300 first recorded use of lenses for eyeglasses

1304 Theodoric of Freiberg explained the water-droplet origins of rainbows

~1500 Leonardo Da Vinci mentioned diffraction in his notebooks

1608 Hans Lippershey makes first telescope after two children playing in his shop put two lenses in front of each other

1609 Galileo produces telescope of power of 30x

1609 Zacarias Joannides made the first microscope. 1620 Willebrord Snell van Royen discovered the law of refraction

1637 Descartes derived the law of refraction theoretically

1663 Robert Boyle first observed interference rings, now known as Newton's rings.

1666 Newton observes spectrum obtained from a prism; publishes Principia

1678 Huygens proposed wave theory of light

1729 Pierre Bouger notices attenuation of light as it passes through successive thicknesses of glass

1733 Joseph Priestly, father of chemistry in America, born

1735 Torbern Bergman born, father of qual and quant inorganic analysis

1743 Antoine Lavoiser, father of modern chemistry born

1750 someone tells Ben Franklin to "go fly a kite"

1752 Thomas Melville writes of yellow light in flame when sea salt mixed with alcohol

1760 Johann Lambert gives mathematical formula to Bouger

1776 Alessandro Volta notes different colors when using different sparking materials

1786 J.B.J. Fourier born

1778 Joseph Louis Gay-Lussac born, father of organic analysis

1791 Michael Faraday born

1800 F.W. Herschel notes that different amounts of heat passed through different colored glasses

1800 Thomas Young demonstrates wave properties of light by diffraction

1801 J.W. Ritter discovers UV

1802 W.H. Wollaston observes dark lines in spectrum from prism (absorption)

1806 John Dalton proposes atomic theory. Daltonism explained.

1817 Josef Fraunhofer maps details of absorption lines in solar spectrum

1826 Balard discovered the photo-sensitivity of silver bromide

1826 W.H.F. Talbot notices different salts yield different colored flames

1838 W.A. Lampadius determines Fe and Ni in Co ores by comparing colors with standard solutions

1850 J.J. Foucault measures speed of light in water

1852 August Beer shows logarithmic relation of Lambert

1852 G.G. Stokes used complementary filters to prove absorption at 1 and emission at 2 (nonresonance luminescence)

1852 E. Bequerel and J.W. Draper photograph solar spectrum

1852 Charles Wheatstone makes drawing of spark spectrum

1853 A. Muller & J. Duboscq use comparator for matching colors by adjusting solution thicknesses

1859 G. Kirchoff and R.W. Bunsen are the first to say that elements have both characteristic absorption and emission spectra

1859 A.J. Angstrom measures ls in a flame and solar spectrum and compares the two

1864 Walther Nernst born, father of electroanalytical chemistry

1864 James Clark Maxwell presented the electromagnetic theory of light

1868 J.N. Lockyer discovers Helium in solar spectrum and in 1873 describes "long" and "short" lines, the first quant work in spectroscopy

1873 Maxwell presented his "Treatise on Electricity and Magnetism"

1877 Gouy invented the first pneumatic nebuliser for introducing liquids into flames

1881 George Stoney proposes that electricity is carried by particles

1882 H.A. Rowland shows that large concave reflection grating can be used for focusing & dispersing

1885 J.J. Balmer develops empirical relationship for Hydrogen spectrum

1886 Eugene Goldstein observes "canal" rays

1887 Heinrich Hertz is first to observe photoelectric effect

1889 H. Ebert develops plane grating optical arrangement

1891 - Gabriel Lippmann made the first colour photographic plate

1891 A.A. Michelson invents interferometer (1907 Nobel Prize in Physics)

1893 V Schumann studied the "vacuum" ultraviolet

1895 W.C. Roentgen discovers x-rays

1896 Zeeman sees splitting of lines in magnetic field

1897 John J. Thompson measures m/e of electron

1900 A. Konig and F.F. Matens develop visible spectrometer

1900 Max Planck proposes quantum theory

1900 William Coblentz takes IR spectra of organics

1902 H.A. Lorentz and P. Zeeman Nobel Prize for discovery of the splitting of spectral lines in magnetic

1903 Mikhial Tswett separates plant pigments with adsorption chromatography

1905 Albert Einstein explains photoelectric effect [A. Einstein, Physikalische Zeitschrift 18, 121 (191]7)

1909 Robert Millikan determines charge on electron using oil drop experiment

1909 Roberts, Pollack, and Leonard do photographic quant work

1911 E. Rutherford, H. Geiger, and E. Marsden discover nucleus of the atom

1913 Neils Bohr proposes "solar system" model ofthe atom

1916 Millikan's systematic studies confirm Einstein's theory on photoelectric effect

1918 Max Plank Nobel Prize in Physics

1919 J. Stark discovery of the splitting of spectral lines in electric fields

1920 W.F. Meggers and P.D. Foote invent microphotometer

1922 N. Bohr, Nobel Prize in Physics, for being the first to link the regularities of spectral lines to the quantum structure of atoms

1923 A. Smekal publishes theoretical foundation of Raman spectroscopy

1924 Pauli postulates nuclear magnetic moments

1926 W. Heisenberg and E. Schrodinger develop wave mechanics

1928 C.V. Raman sees nonresonant scattering (Nobel Physics Prize in 1930)

1929 Lundegardh is first to do quant work with flame photometer

1932 James Chadwick discovers the neutron

1933 C.E. Gleeton and N.H. Williams perform first microwave absorption experiments

1933 Nobel Prize in Physics to P.A.M. Dirac and E. Schrodinger for their contributions to the quantum theory of atoms

1935 Zablonski publishes energy level diagram for molecular luminescence

1938 H.M. Randall and F.A. Firestone use far IR for rotation spectroscopy

1940 Beckman Company begins marketing DU Quartz Spectrophotometer

1942 A.J.P. Martin and R.L.M. Synge develop liquid-liquid chromatography

1944 G.N. Lewis and M. Kasha introduce 5:5:2 EPA for use in phosphorimetry

1945 Felix Block and E.M. Purcell see emission and absorption, respectively, when observing nuclear magnetic resonance

1945 Nobel Prize in Physics to W. Pauli for discovering the quantum exclusion principle

1949 W.D. Knight observes NMR chemical shifts

1949 Peter Fellgett performs Fourier transform of an interferrogram

1949 John White and Max Listen develop double beam optical null IR spectrometer

1951 H.V. Malmstadt begins career at University of Illinois

1951 - E M Purcell and R V Pound first observed net induced emission

1952 A.J. James and A.J.P. Martin develop gas chromatography

1954 Nobel Prize in Chemistyr to Linus Pauling for his research into the nature of the chemical bond

1955 Alan Walsh develops atomic absorption spectroscopy

1955 W.C. Wiley and I.H. McLaren develop time-of-flight mass spectrometer

1955 W. Paul and M. Rather develop quadrupole mass spectrometer

1955 W.E. Lamb, Jr. (Nobel Prize in Physics) for discovering the fine structure splitting in the first excited state of atomic hydrogen

1958 C. Townes(1964 Nobel Prize in Physics), A.L. Schalow (Nobel Physics Prize 1981), and T.H. Maiman develop laser

1959 Digital Equipment Corp. introduces PDP-1

1959 E.R. Ratmond & I.J. Lowe recognize significance of "magic angle" spinning for solid state NMR

1961 B.V. L'vov develops carbon rod furnace

1962 F.J. McClung and R.W. Hellwarth develop pulsed laser

1963 C. Th. J. Alkemade shows that fluorescence of metals can be stimulated in a flame

1964 J.D. Winefordner and T.J. Vickers develop atomic fluorescence spectroscopy

1964 Stanley Greenfield performs first ICP-AES

1964 V.A. Fassel and P.W.J.M. Boumans help with early refinements of ICP

1964 McCormack, Tong, and Cooke develop microwave plasma detector for gas chromatography

1964 A. Savitsky and M.C.E. Golay introduce numerical smoothing

1965 J.B. Willis introduces nitrous oxide-acetylene flame

1965 S. Greenfield invented 'high-power' ICP

1965 S.R. Koirtyohann & E.E. Pickett describe use of hydrogen continuum for background correction

1966 P.P. Sorokin and J.R. Lankard develop dye laser

1966 A. Kastler, Nobel Prize in Physics for for the development of optical pumping of atoms

1966 Nobel Prize in Chemistry to R.S. Mulliken for his contribution to molecular spectroscopy concerning the understanding of chemical bonds and the electronic structure of molecules by the molecular orbital theory

1967 W. Grimm invented his glow discharge source

1968 T. Kuwana develops first spectroelectrochemical apparatus

1968 Massman develops simpler furnace for AA

1968 W. Snelleman introduces wavelength modulation background correction

1968 R. Mavrodineau and R.C. Hughes publish several optical systems for multielement AA

1969 W. Holak describes arsine generation analysis

1969 V.A. Fassel and P.W.J.M. Boumans developed "low-power" ICP

1971 Intel Corp. introduces MCS-4 microprocessor

1971 Nobel Prize in Chemistry to G. Herzberg for his contribution to molecular spectroscopy and the understanding of electronic structure and geometry of molecules, particularly free radicals

1972 Gary Horlick paper on use of Fourier transforms in spectroscopy using digital data handling of spectra

1973 Charlotte E. Moore published extensive tables of atomic energy levels

1975 A.L. Gray develops ICP-MS

1975 J. Ruzicka and E.H. Hansen develop flow injection analysis

1976 C.I.M. Beenakker develops TM010 cavity for microwave plasmas

1976 J. Schaefer & E.O. Stejskal perform key experiments making high resolution solid state NMR feasible

1977 J.P. Walters publishes detailed study of HV spark

1977 O'Haver, Harnly, and Zander develop 16 channel multielement AA

1978 M.P. Fuller and P.J. Griffiths develop diffuse reflectance FTIR

1979 C.G. Enke and R.A. Yost develop triple quadrupole for MS-MS

1981 W. Slavin, D.C. Manning, and G.R. Carnick develop Stabilized Temperature Platform Furnace

1981 N. Bloembergen, Nobel Prize in Physics for his contributions to nonlinear optics

1983 S.B. Smith & G.M. Hieftje introduce pulsed hollow cathode background correction method for AA

1989 H.G. Dehmelt and W. Paul, Nobel Prize in Physics for invention of the ion trap

1991 Nobel Prize in Chemisty to R.R. Ernst for the development of high resolution nuclear magnetic resonance (NMR) spectroscopy

1999 A. Zewail (Nobel Prize in Physics) for studies of the transition states of chemical reactions using femtosecond spectroscopy


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